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Pocket PCs can fall into a couple of different categories. There are true, or traditional, Pocket PCs that are essentially hand-held computers. But there are also Pocket PCs that are now smartphones. The latter has come about fairly recently and was launched with a tremendous amount of buzz. These devices may differ in hardware functionality (some have phone capability and some do not). That notwithstanding, the devices all utilize the Windows Mobile operating system. Consequently, I will cover both true Pocket PCs and smartphones in this section. Pocket PCs are manufactured by a number of different companies, including

These materials (trade names: Epichlomer, Herclor, Hydrin) have good resistance to fuel, oil, ozone, and heat combined with low-temperature exibility and resistance to vapor permeation by air, hydrocarbons, and uorocarbons. Polyoxymethylene, also referred to as acetal resin or POM, is obtained either by anionic polymerization of formaldehyde or cationic ring-opening copolymerization of trioxane with a small amount of a cyclic ether or acetal (e.g., ethylene oxide or 1,3-dioxolane) [Cherdron et al., 1988; Dolce and Grates, 1985; Yamasaki et al., 2001]. The properties and uses of POM have been discussed in Sec. 5-6d. Both anionic and cationic initiation are used to cure (polymerize and crosslink) epoxy resins (Sec. 2-12d) by ROP of the oxirane end groups. Photochemical cationic initiation (Sec. 5-2a-4) is important in various coating applications (3-4c) [Decker et al., 2001]. 7-3 LACTAMS The polymerization of lactams (cyclic amides) can be initiated by bases, acids, and water [Reimschuessel, 1977; Sebenda, 1976, 1978; Sekiguchi, 1984]. Initiation by water, referred to as hydrolytic polymerization, is the most often used method for industrial polymerization of lactams. Anionic initiation is also practiced, especially polymerization in molds to directly produce objects from monomer. Cationic initiation is not useful because the conversions and polymer molecular weights are considerably lower.

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= (1 -

7-50

Nylon 6 is produced commercially, accounting for almost one-third of all polyamides (Sec. 2-8f). Nylons 11 and 12 are specialty polyamides, which nd use in applications requiring higher moisture resistance and hydrolytic stability. Lactams are named in several ways. They are named as alkanolactams by the IUPAC substitutive system, such as 3-propanolactam, 4-butanolactam, 5-pentanolactam, and 6-hexanolactam, respectively, for the 4-, 5-, 6-, and 7-membered rings, respectively. An alternate IUPAC method, the specialist heterocyclic nomenclature system, names these lactams as 2-azetidinone, 2-pyrrolidinone, 2-piperidinone, and hexahydro-2H-azepin-2-one, respectively. These lactams are also known by the trivial names b-propiolactam, a-pyrrolidone (g-butyrolactam), a-piperidone (d-valerolactam), and E-caprolactam, respectively.

A variety of protonic and Lewis acids initiate the cationic polymerization of lactams [Bertalan et al., 1988a,b; Kubisa, 1996; Kubisa and Penczek, 1999; Puffr and Sebenda, 1986; Sebenda, 1988]. The reaction follows the mechanism of acid-catalyzed nucleophilic substitution reactions of amides. More speci cally, polymerization follows an activated monomer mechanism. Initiation occurs by nucleophilic attack of monomer on protonated (activated) monomer (XXIV) to form an ammonium salt (XXV) that subsequently undergoes proton exchange with monomer to yield XXVI and protonated monomer. The conversion of XXIV to XXV involves several steps attachment of nitrogen to C , proton transfer from

7-51

the ordinary derivative with respect to evaluated a t t = 0. Let the contaminating = 6(z), then we recover the influence curve distribution be In particular, for an M-estimator, i.e. for the functional defined by

Covering every model of available Pocket PC would not be prudent in this book. Therefore, only the most popular and well-known devices will be discussed.

one N to the other N, ring opening of the HO-containing ring, and transfer from HO C to N with formation of XXV. Some literature references present variations of the preceding equation whereby protonation of lactam is shown as occurring at nitrogen. This does not correspond to the generally accepted mechanism for acid-catalyzed substitution reactions of amides, such as hydrolysis of acetamide. The available data on such reactions are consistent with protonation occurring almost exclusively at the carbonyl oxygen [Lowry and Richardson, 1987]. Propagation follows in a similar manner as a nucleophilic attack by the primary amine end group of a growing polymer chain (XXVII) on protonated monomer to yield XXVIII,

(n 1)

1-7

evaluated a t = 0,

These polymers do not contain a functional group within the polymer chain but are classi ed as condensation polymers, since water is split out during the polymerization process. Another example is poly( p-xylene), which is produced by the oxidative coupling (dehydrogenation) of p-xylene:

1-8

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